Acrylonitrile → 3-[(3-Hydroxypropyl)amino]propanenitrile

HRID 328182ノート

反応式

HRID 328182 の反応式
[NH2:1][CH2:2][CH2:3][CH2:4][OH:5].[C:6](#[N:9])[CH:7]=[CH2:8]>>[C:6]([CH2:7][CH2:8][NH:1][CH2:2][CH2:3][CH2:4][OH:5])#[N:9]

参加物

3

反応物 2

HCID 7855AcrylonitrileHCID 90863-Amino-1-propanol

生成物 1

HCID 135569403-[(3-Hydroxypropyl)amino]propanenitrile

実験手順

A solution of 75 g. (1 mole) of 3-aminopropanol is stirred while 54 g. (1 mole) of acrylonitrile is added dropwise. After being allowed to stand at room temperature for several hours and preferably overnight, the reaction mixture is concentrated under reduced pressure at 50° yielding 3-(2-cyanoethyl)aminopropanol.

後処理

  1. concentrationthe reaction mixture is concentrated under reduced pressure at 50°

出典と根拠

ORDレコード
ord-ec213696efae4142b407e4af2116f5ac
出典データセット
uspto-grants-1977_04
特許番号
US04016209

反応ノート

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