Palmitoyl chloride → N-methyl-N-(2-palmitoyloxyethyl)benzamide

HRID 328441

反応式

HRID 328441 の反応式
[CH3:1][N:2]([CH2:11][CH2:12][OH:13])[C:3](=[O:10])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.[C:14](Cl)(=[O:30])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29]>>[CH3:1][N:2]([CH2:11][CH2:12][O:13][C:14](=[O:30])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29])[C:3](=[O:10])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1

参加物

3

反応物 2

HCID 8206Palmitoyl chlorideHCID 4047264N-(2-hydroxyethyl)-N-methylbenzamide

生成物 1

HCID 21441878N-methyl-N-(2-palmitoyloxyethyl)benzamide

実験手順

N-methyl-N-(2-palmitoyloxyethyl)benzamide was prepared by the procedure of example 1 from 18 gms. (0.1 mole) of N-methyl-N-(2-hydroxyethyl)benzamide and 26 gms. (0.1 mole) of palmitoyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

後処理

  1. customN-methyl-N-(2-palmitoyloxyethyl)benzamide was prepared by the procedure of example 1 from 18 gms

出典と根拠

ORDレコード
ord-a22d8476e6334d6093f69be5744eccf3
出典データセット
uspto-grants-1977_04
特許番号
US04017522

関連ノート

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