反応式
[NH2:1][CH2:2][C:3]([OH:5])=[O:4].C(=O)([O-])[O-].[Mg+2:10].[Cl-].Cl[O-].[Al+3].Cl[O-].Cl[O-]>O>[NH2:1][CH2:2][C:3]([O-:5])=[O:4].[Mg+2:10].[NH2:1][CH2:2][C:3]([O-:5])=[O:4]参加物
6
反応条件
- 温度
- 75 °C
実験手順
Magnesium glycinate was prepared by reacting 4 grams of glycine with 2.5 grams of basic magnesium carbonate (26.3% Mg) in 30 grams of water while agitating at 75° C. for one half hour. The cooled mixture was then added to 77 grams of zirconyl chloride (13.6% Zr) with stirring. To the above solution 100 grams of 50% aluminum chlorhydroxide (12.5% Al) was added with agitation. The mixture was heated at 85° C. for 20 minutes. The product was then evaporated at 53° C. under a vacuum of 200 mm of Hg and contained 15.8% Al, 13.6% Mg. 5.3% glycine and 22.1% Cl.
後処理
- stirringwith stirring
- temperatureThe mixture was heated at 85° C. for 20 minutes
- customThe product was then evaporated at 53° C. under a vacuum of 200 mm of Hg
出典と根拠
- ORDレコード
- ord-f3633a8a53cf4448a4418701373d167d
- 出典データセット
- uspto-grants-1977_04
- 特許番号
- US04017599
関連ノート
読み込み中…