Calcium Chloride → HCID 21439120、化合物

HRID 329333

反応式

HRID 329333 の反応式
[O:1]=[C:2]1[C:8]2[CH:9]=[CH:10][C:11]([CH:13]([CH3:17])[C:14]([O-:16])=[O:15])=[CH:12][C:7]=2[CH:6]=[CH:5][C:4]2[CH:18]=[CH:19][CH:20]=[CH:21][C:3]1=2.[Na+].[Cl-].[Ca+2:24].[Cl-]>O>[O:1]=[C:2]1[C:8]2[CH:9]=[CH:10][C:11]([CH:13]([CH3:17])[C:14]([O-:16])=[O:15])=[CH:12][C:7]=2[CH:6]=[CH:5][C:4]2[CH:18]=[CH:19][CH:20]=[CH:21][C:3]1=2.[Ca+2:24].[O:1]=[C:2]1[C:8]2[CH:9]=[CH:10][C:11]([CH:13]([CH3:17])[C:14]([O-:16])=[O:15])=[CH:12][C:7]=2[CH:6]=[CH:5][C:4]2[CH:18]=[CH:19][CH:20]=[CH:21][C:3]1=2

参加物

4

反応物 2

HCID 5284359Calcium ChlorideHCID 23670418sodium 2-(5-oxo-5H-dibenzo[a,d]cyclohepten-2-yl)propionate

生成物 1

HCID 21439120HCID 21439120、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒2 回

実験手順

25.2 G. of sodium 2-(5-oxo-5H-dibenzo[a,d]cyclohepten-2-yl)propionate in 300 ml. of water is added to a mixture of 5.55 g. of calcium chloride in 300 ml. of water, and the mixture is allowed to stand for 12 hrs. at room temperature. The mixture is then filtered, and the filtered salt washed several times with portions of ice cold water. The washed salt is dried under vacuum to yield calcium 2-(5-oxo-5H-dibenzo[a,d]cyclohepten-2-yl)propionate.

後処理

  1. customat room temperature
  2. filtrationThe mixture is then filtered
  3. washthe filtered salt washed several times with portions of ice cold water
  4. customThe washed salt is dried under vacuum

出典と根拠

ORDレコード
ord-5b5b2fc142994dc49ee144bd0c4aa90e
出典データセット
uspto-grants-1977_04
特許番号
US04020094

関連ノート

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