Acetic Acid → Tetraethylammonium acetate

HRID 332632

反応式

[OH-].[CH2:2]([N+:4]([CH2:9][CH3:10])([CH2:7][CH3:8])[CH2:5][CH3:6])[CH3:3].[C:11]([OH:14])(=[O:13])[CH3:12]>>[C:11]([O-:14])(=[O:13])[CH3:12].[CH2:2]([N+:4]([CH2:9][CH3:10])([CH2:7][CH3:8])[CH2:5][CH3:6])[CH3:3]

参加物

反応物 2

HCID 176Acetic Acid

HCID 6509Tetraethylammonium Hydroxide

生成物 1

HCID 102017Tetraethylammonium acetate

実験手順

Into an eggplant-shaped flask, an aqueous tetraethylammonium hydroxide solution (1 mol) was charged, and while it was cooled to maintain room temperature, acetic acid (1 mol) was added to obtain tetraethylammonium acetate. Then, ethylene glycol was added as a solvent so that it became a predetermined concentration, and by means of an evaporator, water was distilled off to obtain a solution comprising 50% of tetraethylammonium acetate and 50% of ethylene glycol.

後処理

temperaturewhile it was cooled

出典と根拠

ORDレコード: ord-c1fbea0ea0e64df0a323060c542a36b5
出典データセット: uspto-grants-2014_11
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08877825B2

反応式

参加物

反応物 2

生成物 1

実験手順

後処理

出典と根拠

関連ノート