(3-Aminopropyl)triethoxysilane → Magnesium Acetate

HRID 333524

反応式

HRID 333524 の反応式
O.O.O.O.[C:5]([O-:8])(=[O:7])[CH3:6].[Mg+2:9].[C:10]([O-:13])(=[O:12])[CH3:11].NCCC[Si](OCC)(OCC)OCC.[SiH4].[Mg]>O>[C:5]([O-:8])(=[O:7])[CH3:6].[Mg+2:9].[C:10]([O-:13])(=[O:12])[CH3:11]

参加物

6

反応物 4

HCID 13521(3-Aminopropyl)triethoxysilaneHCID 23953Silane2 回HCID 134717Magnesium Acetate TetrahydrateHCID 5462224Magnesium

生成物 1

HCID 8896Magnesium Acetate

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

An aqueous magnesium acetate solution was prepared by adding 1.07 g of magnesium acetate tetrahydrate as a Group 2 or 3 element compound to 30 g of ion-exchanged water and then stirring this solution with a homomixer T. K. ROBOMIX (manufactured by PRIMIX Corporation). Then, 0.44 g of 3-aminopropyltriethoxysilane (KBE-903 manufactured by Shin-Etsu Chemical Co., Ltd.) as a silane coupling agent was gradually added to the aqueous solution. This mixture was subsequently stirred for 5 hours to induce hydrolysis and a condensation reaction of the silane coupling agent, thereby producing a suspension containing a composite compound which contained magnesium and silicon.

後処理

  1. stirringThis mixture was subsequently stirred for 5 hours
  2. customhydrolysis
  3. customproducing a suspension
  4. additioncontaining a composite compound which

出典と根拠

ORDレコード
ord-95f51b42eeec48c1a080afb136811dd8
出典データセット
uspto-grants-2014_11
特許番号
US08883276B2

関連ノート

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