Formic Acid → HCID 178420610、化合物

HRID 33818

反応式

HRID 33818 の反応式
[N:1]1[C:6](C=O)=[CH:5][CH:4]=[CH:3][C:2]=1C=O.[NH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.C(O)=O>C(O)C>[C:12]1([N:11]=[C:6]2[CH2:5][CH:4]=[CH:3][C:2](=[N:11][C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)[NH:1]2)[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

参加物

5

反応物 3

HCID 284Formic AcidHCID 6115AnilineHCID 794852,6-Diformylpyridine

生成物 1

HCID 178420610HCID 178420610、化合物

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

2,6-pyridine dicarboxaldehyde (0.3071 g, 2.3 mmol) was added to a solution of aniline (0.5292 g, 5.7 mmol) in absolute ethanol (20 mL) at room temperature. 0.5 mL of formic acid was then added to the above solution. The mixture was stirred at room temperature for 65 hours. The product was filtered, washed with cold ethanol and dried in a vacuum oven (50° C.) overnight. Yield 0.2245 g (34.2%).

後処理

  1. filtrationThe product was filtered
  2. washwashed with cold ethanol
  3. customdried in a vacuum oven (50° C.) overnight

出典と根拠

ORDレコード
ord-21efaacccac443d7a83aa3e70255ab54
出典データセット
uspto-grants-2008_09
特許番号
US07429684B2

関連ノート

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