Formic Acid → HCID 178420610、化合物
反応式
[N:1]1[C:6](C=O)=[CH:5][CH:4]=[CH:3][C:2]=1C=O.[NH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.C(O)=O>C(O)C>[C:12]1([N:11]=[C:6]2[CH2:5][CH:4]=[CH:3][C:2](=[N:11][C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)[NH:1]2)[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1参加物
5
実験手順
2,6-pyridine dicarboxaldehyde (0.3071 g, 2.3 mmol) was added to a solution of aniline (0.5292 g, 5.7 mmol) in absolute ethanol (20 mL) at room temperature. 0.5 mL of formic acid was then added to the above solution. The mixture was stirred at room temperature for 65 hours. The product was filtered, washed with cold ethanol and dried in a vacuum oven (50° C.) overnight. Yield 0.2245 g (34.2%).
後処理
- filtrationThe product was filtered
- washwashed with cold ethanol
- customdried in a vacuum oven (50° C.) overnight
出典と根拠
- ORDレコード
- ord-21efaacccac443d7a83aa3e70255ab54
- 出典データセット
- uspto-grants-2008_09
- 特許番号
- US07429684B2
反応ノート
読み込み中…