Hydrochloric Acid → HCID 178418457、化合物

HRID 3391

反応式

HRID 3391 の反応式
[C:1]([C:4]1[CH:5]=[C:6]([CH:8]=[C:9]([C:11](=[O:13])[CH3:12])[CH:10]=1)[NH2:7])(=[O:3])[CH3:2].[C:14]([NH:16][C:17]([NH2:19])=[NH:18])#[N:15].[ClH:20]>O>[ClH:20].[C:1]([C:4]1[CH:5]=[C:6]([NH:7][C:14]([NH:16][C:17]([NH2:19])=[NH:18])=[NH:15])[CH:8]=[C:9]([C:11](=[O:13])[CH3:12])[CH:10]=1)(=[O:3])[CH3:2]

参加物

5

反応物 3

HCID 313Hydrochloric AcidHCID 463010Cni H1894HCID 178418324HCID 178418324、化合物

生成物 1

HCID 178418457HCID 178418457、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Compound No. 12. A suspension of 3,5-diacetylaniline (0.531 g) in water (8 mL) was treated with cyanoguanidine (0.285 g) and conc. HCl (0.25 mL) and heated at reflux. After 6 hr the mixture was cooled and concentrated and 0.248 g of off-white solid was filtered out and dried to give N-(3,5-diacetylphenyl)biguanide hydrochloride, mp 260°-70° C. (dec).

後処理

  1. temperatureheated
  2. temperatureat reflux
  3. temperatureAfter 6 hr the mixture was cooled
  4. concentrationconcentrated
  5. filtration0.248 g of off-white solid was filtered out
  6. customdried

出典と根拠

ORDレコード
ord-705eb0cf3a5441248217ccc079f91152
出典データセット
uspto-grants-1998_03
特許番号
US05733932

関連ノート

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