Stearic Acid → Zinc Stearate

HRID 339439

反応式

HRID 339439 の反応式
[C:1]([OH:20])(=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[OH-].[Zn+2:22].[OH-]>C(O)C>[C:1]([O-:20])(=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[Zn+2:22].[C:1]([O-:20])(=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

参加物

4

反応物 2

HCID 5281Stearic AcidHCID 9812759Zinc Hydroxide

生成物 1

HCID 11178Zinc Stearate

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

反応条件

温度
20 °C

実験手順

1,145 parts of stearic acid is added to 5,000 parts of ethanol, and the mixture is mixed at 75° C. 200 parts of zinc hydroxide is added thereto in small amounts, and the mixture is mixed for one hour from the point of completion of introduction. After the mixing, the mixture is cooled to 20° C., and the product is separated by filtration to remove ethanol and reaction residues. The solid product taken therefrom is dried for 3 hours at 150° C. using a heating type vacuum dryer. The product is removed from the dryer and is cooled naturally. Thus, solid zinc stearate is obtained.

後処理

  1. additionthe mixture is mixed at 75° C
  2. additionin small amounts, and the mixture is mixed for one hour from the point of completion of introduction
  3. customthe product is separated by filtration
  4. customto remove
  5. customethanol and reaction residues
  6. customThe solid product taken therefrom is dried for 3 hours at 150° C.
  7. customThe product is removed from the dryer
  8. temperatureis cooled naturally

出典と根拠

ORDレコード
ord-dddff8b6bfc741e0a5f92a42c195e891
出典データセット
uspto-grants-2014_11
特許番号
US08895216B2

関連ノート

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