N-ethyl-3-methylaniline → Propanamide, N-ethyl-N-(3-methylphenyl)-

HRID 341744

反応式

HRID 341744 の反応式
[CH2:1]([NH:3][C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH3:10])[CH:5]=1)[CH3:2].[C:11](Cl)(=[O:14])[CH2:12][CH3:13]>>[CH2:1]([N:3]([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH3:10])[CH:5]=1)[C:11](=[O:14])[CH2:12][CH3:13])[CH3:2]

参加物

3

反応物 2

HCID 7603N-ethyl-3-methylanilineHCID 62324Propionyl chloride

生成物 1

HCID 44150680Propanamide, N-ethyl-N-(3-methylphenyl)-

実験手順

N-Ethyl-N-(3-methylphenyl)propionamide was prepared on a laboratory scale by acylation of N-ethyl-m-toluidine with propionyl chloride. The reaction was carried out in a 5 litre 3 necked round bottomed flask equipped with a mechanical stirrer, a thermometer (0°-250° C.), an addition vessel and a condenser.

後処理

  1. customequipped with a mechanical stirrer
  2. customa thermometer (0°-250° C.), an addition vessel and a condenser

出典と根拠

ORDレコード
ord-b8e167a762884ac4981728f815e679c1
出典データセット
uspto-grants-1999_01
特許番号
US05856295

関連ノート

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