Methyl p-toluenesulfonate → HCID 86745141、化合物

HRID 345197ノート

反応式

HRID 345197 の反応式
[CH3:1][C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[N:3]=1.[CH3:12][O:13][S:14]([C:17]1[CH:22]=[CH:21][C:20]([CH3:23])=[CH:19][CH:18]=1)(=[O:16])=[O:15]>>[CH3:12][N+:3]1[C:4]2[C:9](=[CH:8][CH:7]=[CH:6][CH:5]=2)[CH:10]=[CH:11][C:2]=1[CH3:1].[CH3:23][C:20]1[CH:21]=[CH:22][C:17]([S:14]([OH:16])(=[O:15])=[O:13])=[CH:18][CH:19]=1

参加物

3

反応物 2

HCID 6645Methyl p-toluenesulfonateHCID 70602-Methylquinoline

生成物 1

HCID 86745141HCID 86745141、化合物

実験手順

2-Methyl-quinoline (71.5 pbw) and methyl-p-toluenesulfonate (102.3 pbw) are heated for about 10 minutes at 100° C. An exothermic reaction sets in, in which the mixture is heated to 180.C. After another 10 minutes the mixture is poured onto acetone, filtered with suction, washed with acetone and dried.

後処理

  1. customAn exothermic reaction sets in, in which the mixture
  2. additionAfter another 10 minutes the mixture is poured onto acetone
  3. filtrationfiltered with suction
  4. washwashed with acetone
  5. customdried

出典と根拠

ORDレコード
ord-d610caabd6674847a09a87c6df6e813e
出典データセット
uspto-grants-1991_10
特許番号
US05055579

反応ノート

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