Ethanolamine → HCID 54121272、化合物

反応式

[CH3:1][C:2]([CH2:7][CH2:8][CH:9]=[C:10]([CH3:27])[CH2:11][CH2:12][CH:13]=[C:14]([CH3:26])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:25])[CH2:19][CH2:20][CH:21]=[C:22]([CH3:24])[CH3:23])=[CH:3][C:4]([OH:6])=O.[CH2:28]([CH2:30][NH2:31])[OH:29]>>[CH3:1][C:2]([CH2:7][CH2:8][CH:9]=[C:10]([CH3:27])[CH2:11][CH2:12][CH:13]=[C:14]([CH3:26])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:25])[CH2:19][CH2:20][CH:21]=[C:22]([CH3:24])[CH3:23])=[CH:3][C:4]([NH:31][CH2:30][CH2:28][OH:29])=[O:6]

参加物

反応物 2

HCID 700Ethanolamine

HCID 543689753,7,11,15,19-Pentamethylicosa-2,6,10,14,18-pentaenoic acid

生成物 1

HCID 54121272HCID 54121272、化合物収率 93%

実験手順

The procedure of Example 1 was repeated except that 7.4 g of 3,7,11,15,19-pentamethyl-2,6,10,14,18-eicosapentaenoic acid and 1.8 ml of ethanolamine were used as starting materials. 7.7 g (yield 93%) of the title compound as a colorless oil was obtained.

出典と根拠

ORDレコード: ord-faf5f28d6dad45d4978b8328ffd4d5ca
出典データセット: uspto-grants-1988_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04762829

反応ノート

読み込み中…