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Cyanuric chloride → 2,4-Dichloro-6-(2,2,6,6-tetramethyl-4-benzoyloxy-piperidin-1-yl)-1,3,5-triazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyanuric chloride | HCID 7954 | — |
| 反応物 | 2,2,6,6-Tetramethyl-4-piperidyl benzoate | HCID 579967 | — |
| 溶媒 | O-Xylene | HCID 7237 | — |
| 生成物 | 2,4-Dichloro-6-(2,2,6,6-tetramethyl-4-benzoyloxy-piperidin-1-yl)-1,3,5-triazine | HCID 19991752 | — |
反応手順
46.1 g of cyanuric chloride and 136.0 g of 2,2,6,6-tetramethyl-4-benzoyloxypiperidine are reacted in 300 ml of xylene as described in Example 1 and worked up. After recrystallization from isopropanol, 2,4-dichloro-6-(2,2,6,6-tetramethyl-4-benzoyloxy-piperidin-1-yl)-1,3,5-triazine are obtained as colorless crystals having a melting point of 145°.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05059689 |
| 出典データセット | uspto-grants-1991_10 |
| ORD ID | ord-9ec55a07da2b40dba42ea0dc185e7fc7 |
| 出典メモ | uspto-grants-1991_10 |