Sodium Hydroxide → HCID 15612245、化合物

HRID 35196ノート

反応式

HRID 35196 の反応式
Cl.[N:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH2:8][C:9]2[CH:18]=[CH:17][C:16]3[C:11](=[CH:12][CH:13]=[C:14]([C:19]([OH:21])=[O:20])[CH:15]=3)[CH:10]=2)[CH:3]=1.[OH-].[Na+]>C(Cl)Cl>[N:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH2:8][C:9]2[CH:18]=[CH:17][C:16]3[C:11](=[CH:12][CH:13]=[C:14]([C:19]([OH:21])=[O:20])[CH:15]=3)[CH:10]=2)[CH:3]=1

参加物

4

反応物 2

HCID 14798Sodium HydroxideHCID 704078322-(3-Pyridylmethyl)naphthalene-6-carboxylic acid hydrochloride

生成物 1

HCID 15612245HCID 15612245、化合物

試薬・触媒・溶媒 1

HCID 6344Dichloromethane溶媒

実験手順

A suspension of 2-(3-pyridylmethyl)naphthalene-6-carboxylic acid hydrochloride in 100 ml of methylene chloride is stirred with a stoichiometric amount of dilute aqueous sodium hydroxide solution until the salt is completely dissolved. The organic layer is separated, washed with water, dried over magnesium sulfate and evaporated to yield 2-(3-pyridylmethyl)naphthalene-6-carboxylic acid.

後処理

  1. dissolutionis completely dissolved
  2. customThe organic layer is separated
  3. washwashed with water
  4. dry with materialdried over magnesium sulfate
  5. customevaporated

出典と根拠

ORDレコード
ord-3af67bb12ea247339371119e2a5e933d
出典データセット
uspto-grants-1988_08
特許番号
US04766127

反応ノート

読み込み中…