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6,7-Dimethoxy-1,2,3,4-Tetrahydroisoquinoline → N-(4-acetoxyphenylacetyl)-1,2,3,4-tetrahydro-6,7-dimethoxyisoquinoline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 6,7-Dimethoxy-1,2,3,4-Tetrahydroisoquinoline | HCID 15623 | — |
| 反応物 | Benzeneacetyl chloride, 4-(acetyloxy)- | HCID 182488 | — |
| 生成物 | N-(4-acetoxyphenylacetyl)-1,2,3,4-tetrahydro-6,7-dimethoxyisoquinoline | HCID 21295827 | — |
反応手順
Using the procedure described in Example 12, 15.0 g of 1,2,3,4-tetrahydro-6,7-dimethoxyisoquinoline was reacted with 4-acetoxyphenylacetyl chloride to give 13.0 g of N-(4-acetoxyphenylacetyl)-1,2,3,4-tetrahydro-6,7-dimethoxyisoquinoline.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04766131 |
| 出典データセット | uspto-grants-1988_08 |
| ORD ID | ord-25ebba0f0ad9463a8279cd0133e1a0db |
| 出典メモ | uspto-grants-1988_08 |