化工社化工社 化学情報印刷レポート · 研究参考用
Imidazole → HCID 23511477、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Imidazole | HCID 795 | — |
| 反応物 | tert-Butyldimethylsilane | HCID 5072427 | — |
| 反応物 | 4-(Hydroxymethyl)-5-methyl-1,3-dioxol-2-one | HCID 10510878 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | HCID 23511477 | HCID 23511477 | — |
反応手順
A solution of 5-methyl-4-hydroxymethyl-2-oxo-1,3-dioxolene (1 mmole) in DMF was treated with tert-butyldimethylsilane (1.2 mmole) and imidazole (2.2 mmole) at 25° C. for 24 h. Extraction and chromatography gave 5-methyl-4-tert-butyldimethylsilyloxymethyl-2-oxo-1,3-dioxolene.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06756360B1 |
| 出典データセット | uspto-grants-2004_06 |
| ORD ID | ord-e740a62547524ca48f9b5d1ddf9d1883 |
| 出典メモ | uspto-grants-2004_06 |