1-Phenylethanol → (1-Chloroethyl)benzene
反応式
[C:1]1([CH:7](O)[CH3:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.N1C(Cl)=NC(Cl)=NC=1[Cl:12]>>[Cl:12][CH:7]([C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)[CH3:8]参加物
3
実験手順
Using a procedure analogous to that of Example 1, 100 g (0.82 mol) of 1-phenylethane-1-ol is reacted with 97.6 g (0.529 mol) of cyanuric chloride over a period of 14 hours at a reaction temperature of 90° C. After phase separation, treatment with sodium hydroxide and purification by distillation, 1-chloro-1-phenylethane having a purity of>99% and containing<0.3% of isomeric alkyl chlorides is obtained.
後処理
- customAfter phase separation, treatment
- customwith sodium hydroxide and purification
- distillationby distillation, 1-chloro-1-phenylethane having a purity of>99%
- additioncontaining<0.3% of isomeric alkyl chlorides
- customis obtained
出典と根拠
- ORDレコード
- ord-06b8f1e0727a4317a83d8d61e641fccb
- 出典データセット
- uspto-grants-2004_06
- 特許番号
- US06756513B2
反応ノート
読み込み中…