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N,N'-Diethylthiourea → HCID 20506556、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N,N'-Diethylthiourea | HCID 2735009 | — |
| 反応物 | 3-Bromo-1,1-diphenylacetone | HCID 2794635 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | HCID 20506556 | HCID 20506556 | — |
反応手順
To a filtered solution of 1.32 g. of 1,3-diethyl-2-thiourea in 25 ml. of acetone is added a filtered solution of 3-bromo-1,1-diphenyl-2-propanone in 25 ml. of acetone. The mixture is allowed to stand, then the solid is collected by filtration, washed with acetone and dried in vacuo, giving 3.73 g. of the desired product, m.p. 174°-176° C. (dec.).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04377589 |
| 出典データセット | uspto-grants-1983_03 |
| ORD ID | ord-2827049d555644459acdb2003933a016 |
| 出典メモ | uspto-grants-1983_03 |