HRID354911

反应详情

EQUATION

反应方程式

HRID 354911 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a filtered solution of 1.32 g. of 1,3-diethyl-2-thiourea in 25 ml. of acetone is added a filtered solution of 3-bromo-1,1-diphenyl-2-propanone in 25 ml. of acetone. The mixture is allowed to stand, then the solid is collected by filtration, washed with acetone and dried in vacuo, giving 3.73 g. of the desired product, m.p. 174°-176° C. (dec.).

WORKUP

后处理

  1. filtrationthe solid is collected by filtration
  2. washwashed with acetone
  3. customdried in vacuo
  4. customgiving 3.73 g