関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Phthalonitrile | HCID 7042 | — |
| 反応物 | HCID 131719385 | HCID 131719385 | — |
| 溶媒 | Ethylene Glycol | HCID 174 | — |
| 生成物 | Gallium phthalocyanine | HCID 136138306 | — |
反応手順
A mixture of 29.1 parts of phthalonitrile, 9.2 parts of gallium trimethoxide, and 150 parts of ethylene glycol was stirred for 24 hours at 200° C. in a nitrogen atmosphere, and the product was filtered. The product was successively washed with N,N-dimethylformamide and then methanol, and dried to provide 23.0 parts of gallium phthalocyanine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05834149 |
|---|
| 出典データセット | uspto-grants-1998_11 |
|---|
| ORD ID | ord-6a845a6c48a24eedaa0d7c9939fef0a4 |
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| 出典メモ | uspto-grants-1998_11 |
|---|
