反应详情

温度

200 °C

A mixture of 29.1 parts of phthalonitrile, 9.2 parts of gallium trimethoxide, and 150 parts of ethylene glycol was stirred for 24 hours at 200° C. in a nitrogen atmosphere, and the product was filtered. The product was successively washed with N,N-dimethylformamide and then methanol, and dried to provide 23.0 parts of gallium phthalocyanine.

1. filtrationthe product was filtered
2. washThe product was successively washed with N,N-dimethylformamide
3. dry with materialmethanol, and dried