反応式
C(N=[N+]=[N-])(=O)[C:2]1[CH:7]=[CH:6][CH:5]=[N:4][CH:3]=1.[N+:12]([C:15]1[CH:16]=[C:17]2[C:21](=[CH:22][CH:23]=1)[NH:20][CH2:19][CH2:18]2)([O-:14])=[O:13].[NH2:24][C:25](N)=[O:26].[ClH:28]>CCOCC>[ClH:28].[N+:12]([C:15]1[CH:16]=[C:17]2[C:21](=[CH:22][CH:23]=1)[N:20]([C:25](=[O:26])[NH:24][C:2]1[CH:3]=[N:4][CH:5]=[CH:6][CH:7]=1)[CH2:19][CH2:18]2)([O-:14])=[O:13]参加物
6
実験手順
This material was prepared from nicotinoyl azide (0.43 g, 2.9 mmol) and 5-nitroindoline (0.38 g, 2.3 mmol), and conversion of the precipitated urea to the salt using excess HCl in ether, following the procedure of Example 2. This gave the title compound (0.64 g, 76%) as a light yellow powder, m.p. 244°-7° C. (dec.).
出典と根拠
- ORDレコード
- ord-aafc92b2637a4682a1f40d81e42fab24
- 出典データセット
- uspto-grants-1998_11
- 特許番号
- US05834494
関連ノート
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