Oxetane → HCID 131720936、化合物

反応式

[O:1]1[CH2:4][CH2:3][CH2:2]1.[C:5]1(=[O:11])[O:10][CH2:9][CH2:8][CH2:7][CH2:6]1.C([Al](CC)CC)C.O>>[C:5]1(=[O:11])[O:10][CH2:9][CH2:8][CH2:7][CH2:6]1.[O:1]1[CH2:4][CH2:3][CH2:2]1

参加物

反応物 3

HCID 10423Oxetane

HCID 10953Delta-Valerolactone

HCID 19429818Triethylalumane--water (1/1)

生成物 1

HCID 131720936HCID 131720936、化合物

実験手順

According to the ratio for charging as described in Table 2, oxetane and delta-valerolactone (referred to as VL in Table and Figure) were mixed, and polymerized in a bulk state at 60° C. for 24 hours using 0.2% by mol of a triethylaluminum-water (1/0.75) based complex as an initiator based on the total amount of the monomers.

後処理

additionwere mixed
custompolymerized in a bulk state at 60° C. for 24 hours

出典と根拠

ORDレコード: ord-5eb6cc29799f4320bb7fc3e47e0a4563
出典データセット: uspto-grants-1998_11
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05834567

反応ノート

読み込み中…