4-Chloroaniline → 4-Chloro-N-[(1H-imidazol-2-yl)methyl]aniline
反応式
[Cl:1][C:2]1[CH:8]=[CH:7][C:5]([NH2:6])=[CH:4][CH:3]=1.[NH:9]1[CH:13]=[CH:12][N:11]=[C:10]1[CH:14]=O>>[Cl:1][C:2]1[CH:8]=[CH:7][C:5]([NH:6][CH2:14][C:10]2[NH:9][CH:13]=[CH:12][N:11]=2)=[CH:4][CH:3]=1参加物
3
実験手順
The title compound was prepared from 4-chloroaniline and 2-imidazole-carboxaldehyde by the same procedure as described in Example 24, part A. The residue was crystallized from ethyl acetate to afford the title compound (1.56 g, 72%) as an off white solid.
後処理
- customThe residue was crystallized from ethyl acetate
出典と根拠
- ORDレコード
- ord-686b47919246456c9585f37f18fabb82
- 出典データセット
- uspto-grants-1998_11
- 特許番号
- US05837702
反応ノート
読み込み中…