4-Mercaptophenol → 4-[(4-Hydroxyphenyl)disulfanyl]phenol

HRID 356842

反応式

HRID 356842 の反応式
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([SH:8])=[CH:4][CH:3]=1>CS(C)=O>[OH:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][S:8][C:5]2[CH:6]=[CH:7][C:2]([OH:1])=[CH:3][CH:4]=2)=[CH:4][CH:3]=1

参加物

3

反応物 1

HCID 2401474-Mercaptophenol

生成物 1

HCID 2806654-[(4-Hydroxyphenyl)disulfanyl]phenol

試薬・触媒・溶媒 1

HCID 679Dimethyl Sulfoxide溶媒

実験手順

p-Hydroxybenzenethiol (25 g) was dissolved in DMSO (155 ml) and the solution was stirred for 4 hours and poured into ice water (1 L). The precipitated crystals were dried under reduced pressure to give bis(p-hydroxyphenyl)disulfide quantitatively.

後処理

  1. customThe precipitated crystals were dried under reduced pressure

出典と根拠

ORDレコード
ord-7085146c16bc4d318e7e2210028e4e8b
出典データセット
uspto-grants-1998_11
特許番号
US05840716

関連ノート

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