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HRID 357724作成日:2026年10月25日

Diisopropyl Ether → (R)-2-bromo-1-(3-chlorophenyl)ethanol

https://huagongshe.com/reaction/357724

反応式

関与物質

役割名称HCID仕込み量
反応物Diisopropyl EtherHCID 7914—
反応物2-Bromo-1-(3-chlorophenyl)ethanolHCID 9964694—
生成物(R)-2-bromo-1-(3-chlorophenyl)ethanolHCID 11075396—

反応手順

Diisopropyl ether was added to a mixture of 100 mg (0.4 mmol) of 2-bromo-1-(3-chlorophenyl)ethanol, 20 mg of TOYOCHIMU LIP (available from Toyobo Co., Ltd.) and 0.3 mmol of each of the various acid anhydrides shown in Table 3 was to make the total volume to 1 ml. These reaction mixtures were respectively allowed to undergo reaction at a temperature of 27° C. for 98 hours. The results are set forth in Table 3.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05841001
出典データセットuspto-grants-1998_11
ORD IDord-8af97dab936b4dbda8044b95a5688946
出典メモuspto-grants-1998_11