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Diisopropyl Ether → (R)-2-bromo-1-(3-chlorophenyl)ethanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Diisopropyl Ether | HCID 7914 | — |
| 反応物 | 2-Bromo-1-(3-chlorophenyl)ethanol | HCID 9964694 | — |
| 生成物 | (R)-2-bromo-1-(3-chlorophenyl)ethanol | HCID 11075396 | — |
反応手順
Diisopropyl ether was added to a mixture of 100 mg (0.4 mmol) of 2-bromo-1-(3-chlorophenyl)ethanol, 20 mg of TOYOCHIMU LIP (available from Toyobo Co., Ltd.) and 0.3 mmol of each of the various acid anhydrides shown in Table 3 was to make the total volume to 1 ml. These reaction mixtures were respectively allowed to undergo reaction at a temperature of 27° C. for 98 hours. The results are set forth in Table 3.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05841001 |
| 出典データセット | uspto-grants-1998_11 |
| ORD ID | ord-8af97dab936b4dbda8044b95a5688946 |
| 出典メモ | uspto-grants-1998_11 |