3-Methyl-2-buten-1-OL → Ethyl 3,3-dimethylpent-4-enoate
反応式
[CH3:1][C:2]([CH3:6])=[CH:3][CH2:4]O.[C:7]([O-:13])([O-])([O:9][CH2:10][CH3:11])[CH3:8]>P(=O)(O)(O)O>[CH3:1][C:2]([CH3:6])([CH:3]=[CH2:4])[CH2:8][C:7]([O:9][CH2:10][CH3:11])=[O:13]参加物
4
実験手順
A mixture of 4.3 g of 3-methyl-2-buten-1-ol, 16.2 g of ethyl orthoacetate and 3 drops of phosphoric acid was reacted as described in Example V A to give 6.15 g (79% yield) of ethyl 3,3-dimethyl-4-pentenoate, b.p. 87°-88°/58 mm.
後処理
- customwas reacted
出典と根拠
- ORDレコード
- ord-3e7cb3b1ca404cda836c93bd7abb5b97
- 出典データセット
- uspto-grants-1991_03
- 特許番号
- US04999451
反応ノート
読み込み中…