Glycerol → Diethylene Glycol Monobutyl Ether

HRID 362741

反応式

HRID 362741 の反応式
C1C(N=NC2C=CC(N/N=[C:21]3/[C:22](S([O-])(=O)=O)=[CH:23][C:24]4[C:29]([C:30]/3=[O:31])=[CH:28][C:27](N)=C(S([O-])(=O)=O)[CH:25]=4)=C3C=2C=CC(S([O-])=O)=C3)=CC=C(S([O-])(=O)=O)C=1.[Na+].[Na+].[Na+].[Na+].O[CH2:53]C(CO)O.[CH2:58]([OH:64])[CH2:59][O:60][CH2:61][CH2:62]O>O>[CH2:30]([O:31][CH2:62][CH2:61][O:60][CH2:59][CH2:58][OH:64])[CH2:29][CH2:28][CH3:27].[CH3:25][CH:24]([CH2:29][C:30]([OH:31])([C:21]#[CH:22])[CH3:53])[CH3:23]

参加物

6

反応物 3

HCID 753GlycerolHCID 8117Diethylene GlycolHCID 178507198HCID 178507198、化合物

生成物 2

HCID 8177Diethylene Glycol Monobutyl EtherHCID 610183,5-Dimethyl-1-hexyn-3-ol

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

A solution containing 2.00 g Food Black 2 (C.I. Food Black 2), 0.08 g LM pectin (Product Name: LM-104AS, The Copenhagen Pectin Factory Ltd.), 5.00 g of glycerol, 5.00 g of diethylene glycol, 8.00 g diethylene glycol mono-n-butyl ether, 0.80 g of Surfynol 465, and 79.12 g of ultrapure water was prepared. The solution was stirred for 2 hours and then filtered through a 5 μm stainless steel mesh.

後処理

  1. filtrationfiltered through a 5 μm stainless steel mesh

出典と根拠

ORDレコード
ord-31f23437de3740f9a4ad67f1c412de66
出典データセット
uspto-grants-1999_02
特許番号
US05871572

関連ノート

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