Thionyl Chloride → 5-Hexylthiophene-2-carboxylic acid chloride
反応式
S(Cl)([Cl:3])=O.[CH2:5]([C:11]1[S:15][C:14]([C:16]([O-:18])=O)=[CH:13][CH:12]=1)[CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]>>[CH2:5]([C:11]1[S:15][C:14]([C:16]([Cl:3])=[O:18])=[CH:13][CH:12]=1)[CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]参加物
3
反応条件
- 温度
- 80 °C
実験手順
10 m of thionyl chloride was added to 1.0 g (4.72×10-3 mol) of 5-hexylthiophene-2-carboxylate and the mixture was stirred for 4 hours at 80° C., followed by removal of excess thionyl chloride, whereby 5-hexylthiophene-2-carboxylic acid chloride was obtained.
後処理
- customfollowed by removal of excess thionyl chloride
出典と根拠
- ORDレコード
- ord-c896d179ae094facb36b1fd49d84e5cd
- 出典データセット
- uspto-grants-1995_05
- 特許番号
- US05413735
反応ノート
読み込み中…