反応式
[CH2:1]([NH:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])[CH2:2][CH2:3][CH2:4][CH3:5].[OH-].[Na+:13].CC(O)C.[C:18](=[S:20])=[S:19]>>[CH2:7]([N:6]([CH2:1][CH2:2][CH2:3][CH2:4][CH3:5])[C:18](=[S:19])[S-:20])[CH2:8][CH2:9][CH2:10][CH3:11].[Na+:13]参加物
5
実験手順
To a 250 mL 3-neck round bottom reaction flask equipped with an overhead stirrer, a thermocouple probe, a reflux condenser, a Claisen adapter, and a 25 mL addition funnel, 30.0 g (0.19 mol) of diamyl amine, 15.3 g of a 50 weight percent NaOH solution (0.19 mol NaOH) and 100 mL reagent 2-propanol was added. 12.5 mL (0.21 mol) carbon disulfide was charged to the addition funnel. Carbon disulfide was added over a half-hour period. The reaction temperature was maintained at 25°-30° C. The product was post-reacted at 25° C. for 1 hour.
後処理
- customTo a 250 mL 3-neck round bottom reaction flask equipped with an overhead stirrer
- additionwas added
- temperatureThe reaction temperature was maintained at 25°-30° C
- customThe product was post-reacted at 25° C. for 1 hour
出典と根拠
- ORDレコード
- ord-51b4618deeff44dd882e3a155e2b5d74
- 出典データセット
- uspto-grants-1999_02
- 特許番号
- US05872286
関連ノート
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