Formic Acid → 3-(3,4-Dimethoxyphenyl)propionic acid

HRID 36413

反応式

HRID 36413 の反応式
FC1C=C[C:5]([CH:8]2[O:13]C(=O)CC(=O)[O:9]2)=CC=1.[CH:16](=O)[C:17]1[CH:26]=[CH:25][C:22]([O:23][CH3:24])=[C:19]([O:20][CH3:21])[CH:18]=1.C(O)=O>C(N(CC)CC)C>[CH3:21][O:20][C:19]1[CH:18]=[C:17]([CH2:16][CH2:5][C:8]([OH:13])=[O:9])[CH:26]=[CH:25][C:22]=1[O:23][CH3:24]

参加物

5

実験手順

5.26 g (0.025 mol) of 2-(4-fluorophenyl)-1,3-dioxane-4,6-dione (m.p.: 166°-167° C.) and 4.15 g (0.025 mol) of veratraldehyde were added to 25 ml of the mixture of formic acid and triethylamine prepared as described in Example 1. The reaction was carried out according to Example 1.

後処理

  1. customprepared

出典と根拠

ORDレコード
ord-95f5fe88279f498a8bab78b6b700accd
出典データセット
uspto-grants-1995_05
特許番号
US05414108

関連ノート

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