反応式
[C:1]([OH:9])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:10]([O:18][CH2:19]COC)(=O)[C:11]1C=CC=CC=1.[CH2:23]([O:27][C:28]1[CH:33]=[CH:32][C:31]([Cl:34])=[CH:30][CH:29]=1)[CH:24]1[O:26][CH2:25]1>COCCO>[C:1]([O:9][CH:24]([CH2:23][O:27][C:28]1[CH:29]=[CH:30][C:31]([Cl:34])=[CH:32][CH:33]=1)[CH2:25][O:26][CH2:11][CH2:10][O:18][CH3:19])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1参加物
5
実験手順
A reaction was conducted as described in Example 6 except that benzoic acid was replaced with the same molar amount of 2-methoxyethyl benzoate, a compound represented by formula (3) where R2 is phenyl and OZ1 is an organic group derived from 2-methoxyethanol, and PGE was replaced with the same molar amount of 4-chlorophenyl glycidyl ether. Desired 1-(4-chlorophenoxymethyl)-2-(2-methoxyethoxy)ethyl benzoate was formed in an analytical yield of 93% and isolated in a yield of 86%.
出典と根拠
- ORDレコード
- ord-ebe83e5750364f8bb5beeb9a960eb2ae
- 出典データセット
- uspto-grants-2000_10
- 特許番号
- US06130346
関連ノート
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