Sodium Hydroxide → HCID 23287656、化合物
反応式
[CH3:1][N:2]([C:14]1[CH:24]=[CH:23][C:17]([C:18]([O:20]CC)=[O:19])=[CH:16][CH:15]=1)[C:3]1[S:4][C:5]2[N:13]=[CH:12][CH:11]=[CH:10][C:6]=2[C:7](=[O:9])[N:8]=1.[OH-].[Na+]>C(O)C>[CH3:1][N:2]([C:14]1[CH:24]=[CH:23][C:17]([C:18]([OH:20])=[O:19])=[CH:16][CH:15]=1)[C:3]1[S:4][C:5]2[N:13]=[CH:12][CH:11]=[CH:10][C:6]=2[C:7](=[O:9])[N:8]=1参加物
4
実験手順
The reaction procedure of Example 116 was followed except that 70 mg g of ethyl 4-[N-methyl-N-(4-oxo-4H-pyrido[3,2-e]-1,3-thiazin-2-yl)amino]benzoate, 0.9 ml of ethanol and 0.9 ml of a 0.25 N aqueous solution of sodium hydroxide were used. As a result, 61 mg of 4-(N-methyl-N-(4-oxo-4H-pyrido[3,2-e]-1,3-thiazin-2-yl)amino]benzoic acid was obtained.
後処理
- customThe reaction procedure of Example 116
出典と根拠
- ORDレコード
- ord-9e68193823f74e2a93b037a21466a820
- 出典データセット
- uspto-grants-2000_10
- 特許番号
- US06133258
反応ノート
読み込み中…