化工社化工社 化学情報印刷レポート · 研究参考用
2-Chloro-N,N-diethylbenzamide → n,n-Diethyl-2-chloro-6-[tris(1-methylethyl)silyl]benzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Chloro-N,N-diethylbenzamide | HCID 82566 | — |
| 反応物 | Triisopropylsilyl chloride | HCID 139400 | — |
| 生成物 | n,n-Diethyl-2-chloro-6-[tris(1-methylethyl)silyl]benzamide | HCID 18630226 | — |
反応手順
The title compound was prepared according to General Method A from the compound of Example e and 1.1 eq triisopropylsilyl chloride. Purification by HPLC using 1:19 ethyl acetate/hexanes gave 5.5 g of the desired product as of a clear oil, a 75% yield.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06133252 |
| 出典データセット | uspto-grants-2000_10 |
| ORD ID | ord-f98a978f36cf430589d464139686e700 |
| 出典メモ | uspto-grants-2000_10 |