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HRID368585

反应详情

EQUATION

反应方程式

HRID 368585 的结构方程式

REACTANTS

反应物

2
结构：CCN(CC)C(=O)c1ccccc1Cl
HCID82566

2-Chloro-N,N-diethylbenzamide

C11H14ClNO

结构：CC(C)[Si](Cl)(C(C)C)C(C)C
HCID139400

Triisopropylsilyl chloride

C9H21ClSi

PRODUCTS

生成物

1
结构：CCN(CC)C(=O)c1c(Cl)cccc1[Si](C(C)C)(C(C)C)C(C)C
HCID18630226

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to General Method A from the compound of Example e and 1.1 eq triisopropylsilyl chloride. Purification by HPLC using 1:19 ethyl acetate/hexanes gave 5.5 g of the desired product as of a clear oil, a 75% yield.

WORKUP

后处理

  1. customThe title compound was prepared
  2. customPurification by HPLC