化工社化工社 化学情報印刷レポート · 研究参考用
Triethylamine → 4-Ethyl-N-methoxy-2,6-dinitroaniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | 4-Chloro-3,5-dinitrotoluene | HCID 78918 | — |
| 反応物 | O-Methylhydroxylamine hydrochloride | HCID 521874 | — |
| 生成物 | 4-Ethyl-N-methoxy-2,6-dinitroaniline | HCID 21329888 | — |
反応手順
Following the same general procedure of Example 2 and using 21.6 g. (0.1 mole) of 2,6-dinitro-4-methylchlorobenzene, 12.5 g. (0.15 mole) of methoxyamine hydrochloride, and 25.25 g. (0.25 mole) of triethylamine, the following additional compound was prepared:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04087460 |
| 出典データセット | uspto-grants-1978_05 |
| ORD ID | ord-e0058999847d4b7e9fc115ed115fe4bb |
| 出典メモ | uspto-grants-1978_05 |