反応式
[C:1]([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([C:10](=[O:12])[CH3:11])[N:5]=1)(=[O:3])C.[BH4-].[Na+].[CH:15](O)(C)C>>[CH3:15][C:10]([CH3:11])([C:6]1[CH:7]=[CH:8][CH:9]=[C:4]([CH2:1][OH:3])[N:5]=1)[OH:12]参加物
4
実験手順
A 250 mL three-necked round bottom flask fitted with magnetic stirrer and nitrogen inlet was charged with 5.0 g (30.6 mmol) of 2,6-diacetylpyridine and 60 mL of anhydrous isopropyl alcohol. To the stirred solution was added 1.16 g (3.06 mmol) of sodium borohydride in three equal portions. The initially colorless solution became yellow and warmed then slowly returned to pale yellow.
後処理
- customA 250 mL three-necked round bottom flask fitted with magnetic stirrer and nitrogen inlet
- temperaturewarmed
出典と根拠
- ORDレコード
- ord-5253aa04c36d4454a7238c8a78fabadd
- 出典データセット
- uspto-grants-1992_11
- 特許番号
- US05166062
関連ノート
読み込み中…