化工社化工社 化学情報印刷レポート · 研究参考用
Cyanuric chloride → 4,6-dichloro-2-ethoxycarbonylmethylamino-S-triazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyanuric chloride | HCID 7954 | — |
| 反応物 | Sodium Bicarbonate | HCID 516892 | — |
| 反応物 | Glycine ethyl ester, hydrochloride | HCID 2723640 | — |
| 溶媒 | 1,4-Dioxane | HCID 31275 | — |
| 生成物 | 4,6-dichloro-2-ethoxycarbonylmethylamino-S-triazine | HCID 14746261 | — |
反応手順
36.9 g of cyanuric chloride, 27.9 g of ethyl glycinate hydrochloride and 33.6 g of sodium bicarbonate were heated under reflux in 200 ml of dioxane for 30 minutes. At the end of this time, the dioxane was removed by distillation under reduced pressure, and a mixture of ethyl acetate and water was added to the resulting residue, after which the mixture was shaken.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05486556 |
| 出典データセット | uspto-grants-1996_01 |
| ORD ID | ord-bd7a9204833e44b8adfa2e160635c080 |
| 出典メモ | uspto-grants-1996_01 |