反应详情

36.9 g of cyanuric chloride, 27.9 g of ethyl glycinate hydrochloride and 33.6 g of sodium bicarbonate were heated under reflux in 200 ml of dioxane for 30 minutes. At the end of this time, the dioxane was removed by distillation under reduced pressure, and a mixture of ethyl acetate and water was added to the resulting residue, after which the mixture was shaken.

1. customAt the end of this time, the dioxane was removed by distillation under reduced pressure
2. additiona mixture of ethyl acetate and water
3. additionwas added to the resulting residue