化工社化工社 化学情報印刷レポート · 研究参考用
Allyl bromide → 2-(2-(Allyloxy)ethoxy)ethanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Allyl bromide | HCID 7841 | — |
| 反応物 | Diethylene Glycol | HCID 8117 | — |
| 溶媒 | NaH THF | HCID 23694757 | — |
| 生成物 | 2-(2-(Allyloxy)ethoxy)ethanol | HCID 84777 | 82% |
反応手順
Diethylene glycol monoallyl ether was prepared by reacting allyl bromide with excess diethylene glycol in THF-NaH (tetrahydrofuran-sodium hydride). The product was obtained in 82% yield after distillation. b.p.=96-99° C./7 mmHg.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08524104B1 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-4e69885985a74b1ca4a5f8fc798f2882 |
| 出典メモ | uspto-grants-2013_09 |