HRID37732

反应详情

EQUATION

反应方程式

HRID 37732 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Diethylene glycol monoallyl ether was prepared by reacting allyl bromide with excess diethylene glycol in THF-NaH (tetrahydrofuran-sodium hydride). The product was obtained in 82% yield after distillation. b.p.=96-99° C./7 mmHg.

WORKUP

后处理

  1. customThe product was obtained in 82% yield
  2. distillationafter distillation