Styrene → GDMA Styrene

HRID 382655

反応式

HRID 382655 の反応式
[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[CH2:9]([O:16][C:17]([CH2:19][SH:20])=[O:18])[CH2:10][O:11][C:12]([CH2:14][SH:15])=[O:13]>>[CH2:10]([O:11][C:12]([CH2:14][SH:15])=[O:13])[CH2:9][O:16][C:17]([CH2:19][SH:20])=[O:18].[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

参加物

3

反応物 2

HCID 7501Styrene2 回HCID 61059Ethylene di(S-thioacetate)

生成物 1

HCID 131721770GDMA Styrene

実験手順

Styrene (481.4 g, 4.62 eq.) was weighed into a 2000 ml, three neck, round bottom flask along with TPO (1.52 g). The flask was sealed with rubber stoppers and placed in a 60° C. oven for approximately 20 minutes. The contents were swirled occasionally until the TPO dissolved into the styrene. The flask was removed from the oven and allowed to cool to less than 40° C. at which point GDMA (518.6 g, 4.467 eq.) was weighed into the flask.

後処理

  1. customThe flask was sealed with rubber stoppers
  2. customplaced in a 60° C.
  3. customfor approximately 20 minutes
  4. customThe flask was removed from the oven

出典と根拠

ORDレコード
ord-518ed148ec3b4428a40b53509f42f34c
出典データセット
uspto-grants-2001_10
特許番号
US06310161B1

関連ノート

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