Iodoethane → Ethyl 1-Boc-3-ethylpiperidine-3-carboxylate

反応式

[CH2:1]([C:3]1([C:16]([O-:18])=[O:17])[CH2:8][CH2:7][CH2:6][N:5]([C:9]([O:11][C:12]([CH3:15])([CH3:14])[CH3:13])=[O:10])[CH2:4]1)[CH3:2].[CH2:19](I)[CH3:20]>>[CH2:1]([C:3]1([C:16]([O:18][CH2:19][CH3:20])=[O:17])[CH2:8][CH2:7][CH2:6][N:5]([C:9]([O:11][C:12]([CH3:14])([CH3:13])[CH3:15])=[O:10])[CH2:4]1)[CH3:2]

参加物

反応物 2

HCID 6340Iodoethane

HCID 756921533-Ethyl-1-[(2-methylpropan-2-yl)oxycarbonyl]piperidine-3-carboxylate

生成物 1

HCID 68429349Ethyl 1-Boc-3-ethylpiperidine-3-carboxylate

実験手順

The target was synthesized as in Production Example 11(1), using 1-tert-butyl 3-ethylpiperidine-1,3-dicarboxylate and ethyl iodide as the raw material.

後処理

customThe target was synthesized as in Production Example 11(1)

出典と根拠

ORDレコード: ord-ced3c0fe4ffe4b6798531c68d940d563
出典データセット: uspto-grants-2013_02
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08367698B2

反応ノート

読み込み中…