tert-Butyl mercaptan → (2'-tert-Butylsulfanylmethyl-6-methoxy-4'-trifluoromethyl-biphenyl-3-yl)-acetic acid ethyl ester

HRID 38690

反応式

HRID 38690 の反応式
[CH2:1]([O:3][C:4](=[O:26])[CH2:5][C:6]1[CH:7]=[C:8]([C:14]2[CH:19]=[CH:18][C:17]([C:20]([F:23])([F:22])[F:21])=[CH:16][C:15]=2[CH2:24]Br)[C:9]([O:12][CH3:13])=[CH:10][CH:11]=1)[CH3:2].[CH3:27][C:28]([SH:31])([CH3:30])[CH3:29]>>[CH2:1]([O:3][C:4](=[O:26])[CH2:5][C:6]1[CH:7]=[C:8]([C:14]2[CH:19]=[CH:18][C:17]([C:20]([F:23])([F:22])[F:21])=[CH:16][C:15]=2[CH2:24][S:31][C:28]([CH3:30])([CH3:29])[CH3:27])[C:9]([O:12][CH3:13])=[CH:10][CH:11]=1)[CH3:2]

参加物

3

反応物 2

HCID 6387tert-Butyl mercaptanHCID 67430388(2'-Bromomethyl-6-methoxy-4'-trifluoromethyl-biphenyl-3-yl)-acetic acid ethyl ester

生成物 1

HCID 67430962(2'-tert-Butylsulfanylmethyl-6-methoxy-4'-trifluoromethyl-biphenyl-3-yl)-acetic acid ethyl ester

実験手順

Prepared according to the procedure described in Example 1, Step 6, using the following starting materials: (2′-bromomethyl-6-methoxy-4′-trifluoromethyl-biphenyl-3-yl)-acetic acid ethyl ester and 2-methyl-2-propanethiol.

後処理

  1. customPrepared

出典と根拠

ORDレコード
ord-d16eb85e0d394f63adbffaa841e2444c
出典データセット
uspto-grants-2013_09
特許番号
US08524748B2

関連ノート

読み込み中…