化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Iodide → HCID 66732740、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Iodide | HCID 5238 | — |
| 反応物 | (1,1'-Biphenyl)-2-ol | HCID 7017 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 1-Octanol, 8-chloro- | HCID 90012 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 66732740 | HCID 66732740 | — |
反応手順
The compound was prepared using essentially the procedure of Preparatory Example 1 with 2-hydroxy biphenyl (40 g.), water (250 g.), sodium iodide (3.5 g.) and sodium hydroxide (37.6 g. of 50% in water). This mixture was heated to 100° C. with agitation and 8-chloro-1-octanol (77.4 g.) was added. The product was recovered essentially as in Preparatory Example 1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08378046B2 |
| 出典データセット | uspto-grants-2013_02 |
| ORD ID | ord-05054416c02248f89e5b132dca5599b6 |
| 出典メモ | uspto-grants-2013_02 |