戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 389654作成日:2026年10月26日

Benzyl mercaptan → 1-Benzylsulfanyl-3-bromo-2-trifluoromethyl-benzene

https://huagongshe.com/reaction/389654

反応式

関与物質

役割名称HCID仕込み量
反応物Benzyl mercaptanHCID 7509—
反応物2-Bromo-6-fluorobenzotrifluorideHCID 2773345—
生成物1-Benzylsulfanyl-3-bromo-2-trifluoromethyl-benzeneHCID 67155259—

反応手順

Phenyl-methanethiol (4.g g, 37.0 mmol) was treated with commercially available 1-bromo-3-fluoro-2-trifluoromethyl-benzene (10.0 g, 41.1 mmol) in close analogy to the procedure described in step 5.3). The crude product (10.5 g) after workup was used as such in the next reaction step without purification by chromatography.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08378092B2
出典データセットuspto-grants-2013_02
ORD IDord-e82cb9c16d524ad382d59b2d011bdb18
出典メモuspto-grants-2013_02