2-Acrylamido-2-methyl-1-propanesulfonic acid → Ammonium acryloyldimethyltaurate

HRID 389787

反応式

HRID 389787 の反応式
COCCOCC[N:8](CCOCCOC)CCOCCOC.[C:23]([NH:27][C:28]([CH3:35])([CH3:34])[CH2:29][S:30]([OH:33])(=[O:32])=[O:31])(=[O:26])[CH:24]=[CH2:25]>>[NH4+:8].[C:23]([NH:27][C:28]([CH3:35])([CH3:34])[CH2:29][S:30]([O-:33])(=[O:31])=[O:32])(=[O:26])[CH:24]=[CH2:25]

参加物

3

反応物 2

HCID 653602-Acrylamido-2-methyl-1-propanesulfonic acidHCID 112414Ethanamine, 2-(2-methoxyethoxy)-N,N-bis[2-(2-methoxyethoxy)ethyl]-

生成物 1

HCID 6850854Ammonium acryloyldimethyltaurate収率 99%

実験手順

A nitrogen purged 50 ml schlenk flask was charged with freshly distilled tris[2-(2-methoxyethoxy)-ethyl]amine (1.69 g, 5.24 mmol) and 2-acrylamido-2-methyl-1-propanesulfonic acid (AMPS) (1.09 g, 5.24 mmol) and stirred at ambient temperature for 8 hr or until completely dissolved. Total dissolution completes formation of the AMPS-ammonium salt monomer as a transparent light amber oil in a 99% yield which was used immediately without further purification.

後処理

  1. customA nitrogen purged 50 ml schlenk flask
  2. dissolutionuntil completely dissolved
  3. dissolutionTotal dissolution
  4. customwas used immediately without further purification

出典と根拠

ORDレコード
ord-f8b9578b9867420d8964739d7569bf17
出典データセット
uspto-grants-2013_02
特許番号
USRE044032E1

関連ノート

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