Methyl iodide → Quinolinium, 1-methyl-, iodide (1:1)
反応式
[N:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1.[CH3:11][I:12]>O1CCOCC1>[I-:12].[CH3:11][N+:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1参加物
4
反応条件
- 温度
- 150 °C
実験手順
N-methylquinolinium iodide (Compound III) was synthesized according to the description in the aforementioned reference. Specifically, 2.4 mL of quinoline and 4 mL of methyl iodide were added to 42 mL of anhydrous dioxane, which was stirred at 150° C. for one hour. Thereafter, it was filtered and thereby a precipitate was collected and then washed with ether and petroleum ether. This was dried and thus N-methylquinolinium iodide (Compound III) was obtained.
後処理
- customN-methylquinolinium iodide (Compound III) was synthesized
- filtrationThereafter, it was filtered
- customa precipitate was collected
- washwashed with ether and petroleum ether
- customThis was dried
出典と根拠
- ORDレコード
- ord-6af5ef6efe2a4092938a0c01e49a2c54
- 出典データセット
- uspto-grants-2013_02
- 特許番号
- US08383792B2
反応ノート
読み込み中…