Methyl cyclohexanecarboxylate → Methyl 1-(iodomethyl)cyclohexanecarboxylate

HRID 393735

反応式

HRID 393735 の反応式
[CH3:1][O:2][C:3]([C:5]1([CH2:11][I:12])[CH2:10][CH2:9]O[CH2:7][CH2:6]1)=[O:4].[CH3:13]OC(C1CCCCC1)=O>>[CH3:1][O:2][C:3]([C:5]1([CH2:11][I:12])[CH2:10][CH2:9][CH2:13][CH2:7][CH2:6]1)=[O:4]

参加物

3

反応物 2

HCID 20748Methyl cyclohexanecarboxylateHCID 227197884-Iodomethyl-tetrahydro-pyran-4-carboxylic acid methyl ester

生成物 1

HCID 58947958Methyl 1-(iodomethyl)cyclohexanecarboxylate収率 100%

実験手順

Prepared according to the method for the preparation of 4-iodomethyltetrahydropyran-4-carboxylic acid methyl ester, from cyclohexane-carboxylic acid methyl ester (10 ml), to give the title compound as a brown gum (20 g, 100%).

後処理

  1. customPrepared

出典と根拠

ORDレコード
ord-ddacfc71a8504682a05627c6e4b3745c
出典データセット
uspto-grants-2004_10
特許番号
US06809100B2

関連ノート

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