Octyltrichlorosilane → HCID 13977504、化合物

HRID 395241

反応式

HRID 395241 の反応式
[C:1]([O-:4])(=[O:3])[CH3:2].[Na+].[CH2:6]([Si:14](Cl)(Cl)Cl)[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13]>CCCCCCC>[CH2:6]([Si:14]([O:4][C:1](=[O:3])[CH3:2])([O:3][C:1](=[O:4])[CH3:2])[O:3][C:1](=[O:4])[CH3:2])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13]

参加物

4

反応物 2

HCID 21354OctyltrichlorosilaneHCID 517045Sodium Acetate

生成物 1

HCID 13977504HCID 13977504、化合物収率 88%

試薬・触媒・溶媒 1

HCID 8900Heptane溶媒

実験手順

In a 1-1 round-bottomed flask were placed first 55 g of anhydrous sodium acetate, and then 500 ml of anhydrous heptane. To the white suspension formed was added 50 g of octyltrichlorosilane. The reaction medium was left under stirring at ambient temperature for 2 h, and then filtered under argon to remove the precipitate. The filtrate was concentrated to eliminate the heptane, giving 54 g (88% yield) of octyltriacetoxysilane as a colorless oil.

後処理

  1. customTo the white suspension formed
  2. waitThe reaction medium was left
  3. filtrationfiltered under argon
  4. customto remove the precipitate
  5. concentrationThe filtrate was concentrated

出典と根拠

ORDレコード
ord-4ac068724ab44b20bce208aa01a6c954
出典データセット
uspto-grants-2003_08
特許番号
US06605423B2

関連ノート

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